殺線威檢測

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GB 5085.3-2007危險(xiǎn)廢物鑒別標(biāo)準(zhǔn) 浸出毒性鑒別

本標(biāo)準(zhǔn)規(guī)定了以浸出毒性為特征的危險(xiǎn)廢物鑒別標(biāo)準(zhǔn)。 本標(biāo)準(zhǔn)適用于任何生產(chǎn)、生活和其他活動中產(chǎn)生固體廢物的浸出毒性鑒別。

GB/T 18412.5-2008紡織品.農(nóng)藥殘留量的測定.第5部分:有機(jī)氮農(nóng)藥

警告——使用GB/T 18412的本部分的人員應(yīng)有正規(guī)實(shí)驗(yàn)室工作的實(shí)踐經(jīng)驗(yàn)。本部分并未指出所有可能的安全問題。使用者有責(zé)任采取適當(dāng)?shù)陌踩徒】荡胧⒈ＷC符合有關(guān)法規(guī)規(guī)定的條件。GB/T 18412的本部分規(guī)定了采用液相色譜-質(zhì)譜/質(zhì)譜（LC-MS/MS）測定紡織品中8種有機(jī)氮農(nóng)藥殘留量的方法。本部分適用于紡織材料及其產(chǎn)品。

GB/T 20772-2008動物肌肉中461種農(nóng)藥及相關(guān)化學(xué)品殘留量的測定.液相色譜-串聯(lián)質(zhì)譜法

本標(biāo)準(zhǔn)規(guī)定了豬肉、牛肉、羊肉、兔肉、雞肉中 461 種農(nóng)藥及相關(guān)化學(xué)品 ( 參見附錄 A 和附錄 E) 殘留量液相色譜 -串聯(lián)質(zhì)譜測定方法。本標(biāo)準(zhǔn)適用于豬肉、牛肉、羊肉、兔肉、雞肉中 461 種農(nóng)藥及相關(guān)化學(xué)品的定性鑒別 ,396 種農(nóng)藥及相關(guān)化學(xué)品殘留量的定量測定。本標(biāo)準(zhǔn)定量測定的 396 種農(nóng)藥及相關(guān)化學(xué)品的方法檢出限為 0.04μg/kg~4.82mg/kg( 參見附錄 A) 。

GB 23200.90-2016食品安全標(biāo)準(zhǔn) 乳及乳制品中多種氨基甲酸酯類農(nóng)藥殘留量的測定 液相色譜—質(zhì)譜法

本標(biāo)準(zhǔn)規(guī)定了乳和乳制品中殺線威、滅多威、抗蚜威、涕滅威、速滅威、蟲威、克百威、甲萘威、呋線威、異丙威、乙霉威、仲丁威、殘殺威和甲硫威14種氨基甲酸酯類農(nóng)藥殘留量的液相色譜—質(zhì)譜檢測方法。本標(biāo)準(zhǔn)適用于純奶、酸奶、奶粉、奶酪和果奶中殺線威、滅多威、抗蚜威、涕滅威、速滅威、蟲威、克百威、甲萘威、呋線威、異丙威、乙霉威、仲丁威、殘殺威和甲硫威殘留量的測定和確證，其他食品可參照執(zhí)行。

GB/T 23208-2008河豚魚、鰻魚和對蝦中450種農(nóng)藥及相關(guān)化學(xué)品殘留量的測定.液相色譜-串聯(lián)質(zhì)譜法

本標(biāo)準(zhǔn)規(guī)定了河豚魚、鰻魚和對蝦中450種農(nóng)藥及相關(guān)化學(xué)品（參加附錄A和附錄E）殘留量液相色譜－串聯(lián)質(zhì)譜測定方法。本標(biāo)準(zhǔn)適用于河豚魚、鰻魚和對蝦中450種農(nóng)藥及相關(guān)化學(xué)品殘留量的定性鑒別，也適用于其中380種農(nóng)藥及相關(guān)化學(xué)品的定量測定。本標(biāo)準(zhǔn)定量測定的380種農(nóng)藥及相關(guān)化學(xué)品的方法檢出限為0.02μg/kg～0.195mg/kg（參見附錄A）。

GB/T 23211-2008牛奶和奶粉中493種農(nóng)藥及相關(guān)化學(xué)品殘留量的測定.液相色譜-串聯(lián)質(zhì)譜法

本標(biāo)準(zhǔn)規(guī)定了牛奶和奶粉中493種農(nóng)藥及相關(guān)化學(xué)品（參加附錄A和附錄E）殘留量液相色譜－串聯(lián)質(zhì)譜測定方法。本標(biāo)準(zhǔn)適用于牛奶中482種農(nóng)藥及相關(guān)化學(xué)品的定性鑒別，441種農(nóng)藥及相關(guān)化學(xué)品的定量測定；適用于奶粉中481種農(nóng)藥及相關(guān)化學(xué)品的定性鑒別，427種農(nóng)藥及其相關(guān)化學(xué)品的定量測定。本標(biāo)準(zhǔn)定量測定的441種農(nóng)藥及相關(guān)化學(xué)品的方法檢出限為0.01μg/L～2.41mg/L（參見附錄A）；定量測定的奶粉中427種農(nóng)藥及相關(guān)化學(xué)品的方法檢出限為0.04μg/kg～8.04mg/kg（參見附錄A）。

NY/T 1453-2007蔬菜及水果中多菌靈等16種農(nóng)藥殘留測定液相色譜.質(zhì)譜.質(zhì)譜聯(lián)用法

本標(biāo)準(zhǔn)規(guī)定了蔬菜、水果中多菌靈等 16 種農(nóng)藥的殘留用液相色譜-質(zhì)譜-質(zhì)譜聯(lián)用測定方法。 本標(biāo)準(zhǔn)適用于蔬菜、水果中多菌靈、殺線威、噻菌靈、滅多威、吡蟲琳、啶蟲脒、嘧菌酯、虱螨脲、多殺菌素、咪鮮胺、氟菌唑、氟苯脲、氟蟲脲、伐蟲脒、霜霉威、氟鈴脲殘留量的測定。 16 種農(nóng)藥的低檢出限為0.01mg/kg～0.10mg/kg。

NY/T 2049-2011香蕉、番石榴、胡椒、菠蘿線蟲防治技術(shù)規(guī)范

本標(biāo)準(zhǔn)規(guī)定了香蕉Musa paradisiaca Linn.、番石榴Psidium guajava L.、胡椒Piper nigrum Linn.與菠蘿Ananas comosus(L.)Merr.線蟲的防治原則、措施和方法。本標(biāo)準(zhǔn)適用于香蕉根結(jié)線蟲(南方根結(jié)線蟲Meloidogyne incognita Chitwood、花生根結(jié)線蟲M.arenaria Chitwood、爪哇根結(jié)線蟲M.javanica Treub、高弓根結(jié)線蟲M.acrita Chitwood、巨大根結(jié)線蟲M.megadora Whitehead）、番石榴根結(jié)線蟲(南方根結(jié)線蟲Meloidogyne incognita Chitwood、湛江根結(jié)線蟲M.zhanjiangensis Liao、番禺根結(jié)線蟲M.panyuensis Liao）、胡椒根結(jié)線蟲(南方根結(jié)線蟲Meloidogyne incognita Chitwood、花生根結(jié)線蟲M.arenaria Chitwood)與菠蘿根結(jié)線蟲(南方根結(jié)線蟲Meloidogyne incognita Chitwood、爪哇根結(jié)線蟲M.javanica Treub)的防治。

SN/T 0134-2010進(jìn)出口食品中殺線威等12種氨基甲酸酯類農(nóng)藥殘留量的檢測方法.液相色譜-質(zhì)譜/質(zhì)譜法

本標(biāo)準(zhǔn)規(guī)定了食品中紗線威、滅多威、抗蚜威、涕滅威、速滅威、克百威、甲萘威、乙硫甲威、異丙威、乙霉威和仲丁威等12中氨基甲酸酯類農(nóng)藥殘留量的液相色譜-質(zhì)譜/質(zhì)譜檢測方法。本標(biāo)準(zhǔn)適用于玉米、糙米、大麥、白菜、大蔥、小麥、大豆、花生、蘋果、柑橘、牛肝、雞腎和蜂蜜中殺線威、滅多威、抗蚜威、涕滅威、速滅威、克百威、甲萘威、乙硫甲威、異丙威、乙霉威和仲丁威殘留量的檢測和確證。

SN/T 0697-2014出口肉及肉制品中殺線威殘留量的測定

本標(biāo)準(zhǔn)規(guī)定了出口肉及肉制品中殺線威殘留量測定的液相色譜-質(zhì)譜/質(zhì)譜和液相色譜檢測方法。本標(biāo)準(zhǔn)適用于出口豬肉、牛肉、羊肉、雞肉、香腸中殺線威殘留量的測定。

SN/T 1017.7-2014出口糧谷中涕滅威、甲萘威、殺線威、惡蟲威、抗蚜威殘留量的測定

SN/T 1017的本部分規(guī)定了出n糧谷中涕滅威、甲萘威、殺線威、惡蟲威、抗蚜威殘留量的液相色譜-質(zhì)譜/質(zhì)譜和液相色譜的測定方法。本部分適用于出口大米、玉米、小麥和大豆中涕滅威、甲萘威、殺線威、惡蟲威、抗蚜威五種氨基甲酸酯類農(nóng)藥殘留量的測定。

SN/T 4428-2016出口油料和植物油中多種農(nóng)藥殘留量的測定 液相色譜-質(zhì)譜/質(zhì)譜法

本標(biāo)準(zhǔn)規(guī)定了出口油料和植物油中多種農(nóng)藥殘留量的液相色譜-質(zhì)譜／質(zhì)譜測定方法。本標(biāo)準(zhǔn)適用于大豆油、玉米油、花生油、橄欖油、菜籽油、棕櫚油、油菜籽、花生、芝麻、瓜子中77種農(nóng)藥殘留量的測定。

HJ 961-2018土壤和沉積物 氨基甲酸酯類農(nóng)藥的測定 液相色譜-三重四極桿質(zhì)譜法

本標(biāo)準(zhǔn)規(guī)定了測定土壤和沉積物中15種氨基甲酸酯類農(nóng)藥的液相色譜-三重四極桿質(zhì)譜法。本標(biāo)準(zhǔn)適用于土壤和沉積物中殺線威、滅多威、二氧威、涕滅威、惡蟲威、克百威、殘殺威、甲萘威、乙硫苯威、抗蚜威、異丙威、仲丁威、甲硫威、猛殺威、棉鈴?fù)?5種氨基甲酸酯類農(nóng)藥的測定。當(dāng)取樣量為10 g，試樣定容體積為1.0 ml，進(jìn)樣體積為1.0 μl時(shí)，15種氨基甲酸酯類農(nóng)藥的方法檢出限為1~2 μg/kg，測定下限為4~8 μg/kg。詳見附錄A。

HJ 1026-2019固體廢物 氨基甲酸酯類農(nóng)藥的測定 液相色譜-三重四極桿質(zhì)譜法

本標(biāo)準(zhǔn)規(guī)定了測定固體廢物及其浸出液中氨基甲酸酯類農(nóng)藥的液相色譜-三重四極桿質(zhì)譜法。本標(biāo)準(zhǔn)適用于固體廢物及其浸出液中殺線威、滅多威、二氧威、涕滅威、惡蟲威、克百威、殘殺威、甲萘威、乙硫苯威、抗蚜威、異丙威、仲丁威、甲硫威、猛殺威、棉鈴?fù)?5種氨基甲酸酯類農(nóng)藥的測定。當(dāng)固體廢物取樣量為10 g，定容體積為5.0 ml，進(jìn)樣體積為1 μl時(shí)，15種氨基甲酸酯類農(nóng)藥的方法檢出限為1.0~2.0 μg/kg，測定下限為4.0~8.0 μg/kg。當(dāng)固體廢物浸出液取樣體積為100 ml，定容體積為5.0 ml，進(jìn)樣體積為1 μl時(shí)，15種氨基甲酸酯類農(nóng)藥的方法檢出限為0.2 μg/L，測定下限為0.8 μg/L。詳見附錄A。

DB53/T 356-2011煙草及煙草制品氨基甲酸酯類農(nóng)藥殘留量的測定液相色譜法氨基甲酸酯類農(nóng)藥殘留量的測定液相色譜法

本標(biāo)準(zhǔn)規(guī)定了煙草及煙草制品中涕滅威、涕滅威砜、涕滅威亞砜、丁酮威、丁酮威砜、丁酮威亞砜、克百威、3-羥基克百威、3-酮克百威、甲硫威、甲硫威砜、甲硫威亞砜、乙硫甲威、乙硫甲威砜、乙硫甲威亞砜、滅多威、抗蚜威、殺線威、速滅威、殘殺威、甲萘威、異丙威、丁苯威、茲克威 24 種氨基甲酸酯類農(nóng)藥殘留量的測定方法。本標(biāo)準(zhǔn)適用于煙草及煙草制品氨基甲酸酯類農(nóng)藥殘留量的測定。

ASTM D7600-2009液相色譜串聯(lián)質(zhì)譜法測定涕滅威、克百威、殺線威及滅多威的標(biāo)準(zhǔn)試驗(yàn)方法

The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl.1.1 This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2 This test method has been developed in support of the National Homeland Security Research Center, US EPA by Region 5 Chicago Regional Laboratory. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1 The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2 The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D7600-2009e1液相色譜串聯(lián)質(zhì)譜法測定涕滅威,克百威,殺線威及滅多威的標(biāo)準(zhǔn)試驗(yàn)方法

The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl. 1.1 This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2 This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1 The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2 The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. TABLE 1 Detection Verification Level and Reporting Range AnalyteDVL (x03BC;g/L)Reporting Range (x03BC;g/L) Aldicarb1001x2013;100 Carbofuran1001x2013;100 Oxamyl1001x2013;100 Methomyl1001x2013;100 TABLE 2 Concentrations of Calibration Standards (PPB) Analyte/Surrogate LV 1LV 2LV 3LV 4

ASTM D7600-2009e2使用液相色譜法/串聯(lián)質(zhì)譜法測定涕滅威, 克百威, 殺線威及滅多威的標(biāo)準(zhǔn)試驗(yàn)方法

5.1x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water.4 5.2x00a0;This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl. 1.1x00a0;This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3x00a0;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. TABLE 1 Detection Verification Level and Reporting Range Analyte DVL (ng/L)x2020; Reporting Range (x03bc;g/L)

ASTM D7600-2009e3使用液相色譜法/串聯(lián)質(zhì)譜法測定涕滅威, 克百威, 殺線威及滅多威的標(biāo)準(zhǔn)試驗(yàn)方法

5.1x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water.4 5.2x00a0;This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl. 1.1x00a0;This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3x00a0;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1x00a0;The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2x00a0;The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D7600-2016采用液相色譜法/串聯(lián)質(zhì)譜法測定涕滅威, 呋喃丹, 殺線威和滅多威的標(biāo)準(zhǔn)試驗(yàn)方法

5.1x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water.4 5.2x00a0;This test method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl, and methomyl. 1.1x00a0;This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this test method. This test method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3x00a0;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1x00a0;The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2x00a0;The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.